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1 article(s) from Allagui, Anis

3D-nanoarchitectured Pd/Ni catalysts prepared by atomic layer deposition for the electrooxidation of formic acid

Loïc Assaud,
Evans Monyoncho,
Kristina Pitzschel,
Anis Allagui,
Matthieu Petit,
Margrit Hanbücken,
Elena A. Baranova and
Lionel Santinacci

Beilstein J. Nanotechnol. 2014, 5, 162–172, doi:10.3762/bjnano.5.16

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Scheme 1: Pd-catalyzed electrooxidation of HCOOH on Pd surfaces.

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Figure 1: Schematic description of the anodic alumina template fabrication and successive functionalization. ...

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Figure 2: (a) In situ QCM measurement of the NiO mass gain during the ALD process. (b) Enlarged view of the m...

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Figure 3: (a) SEM cross section of a NiO layer deposited in AAO membrane. (b) SEM image (obtained in backscat...

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Figure 4: (a) TEM image of NiO nanotubes after alumina template removal. (b) Enlarged view of NiO nanotubes.

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Figure 5: SEM image of Ni layer deposited in an AAO template after 3 h annealing in H₂ at 300 °C of the initi...

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Figure 6: XPS survey spectrum of metallic Ni.

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Figure 7: ALD sequence during Pd deposition from Pd(hfac)₂ and formaldehyde.

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Figure 8: In situ QCM measurements of Pd mass gain during the ALD process for Pd. (a) General evolution and (...

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Figure 9: SEM top views of Pd deposits after 100 ALD cycles onto (a) as-grown NiO and (b) reduced NiO films o...

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Figure 10: X-ray diffractogram of Pd deposited by ALD exhibiting a polycrystalline structure with a preferenti...

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Figure 11: XPS survey spectrum of metallic Pd.

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Figure 12: Cyclic voltammograms of Pd(100 ALD cycles)/Ni(1000 ALD cycles) catalysts in 0.5 M H₂SO₄ without (bl...

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Figure 13: Peak current densities of the electrooxidation of 1 M HCOOH in 0.5 M H₂SO₄ with various Pd contents...

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Figure 14: SEM micrograph of an anodic alumina oxide template. After the electropolishing, a sacrificial film ...

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Published 12 Feb 2014

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